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مقاله Applying full factorial design to the optimization of HدرZSMدر5 zeolite synthesis for methanol dehydration to dimethyl ether تحت word دارای 9 صفحه می باشد و دارای تنظیمات در microsoft word می باشد و آماده پرینت یا چاپ است

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بخشی از متن مقاله Applying full factorial design to the optimization of HدرZSMدر5 zeolite synthesis for methanol dehydration to dimethyl ether تحت word :

سال انتشار: 1390

محل انتشار: هفتمین کنگره ملی مهندسی شیمی

تعداد صفحات: 9

نویسنده(ها):

samaneh hosseini – Chemical Engineering Department, Babol University of Technology, P.O. Box 484, 4714871167 Babol, Iran
majid taghizadeh – Chemical Engineering Department, Babol University of Technology, P.O. Box 484, 4714871167 Babol, Iran
ali eliassi – Chemical Industries Research Department, Iranian Research Organization for Science and Technology (IROST), Tehran, Iran

چکیده:

H-ZSM-5 zeolite was synthesized by hydrothermal method. The effects of different synthesis parameters, including temperature (170190 °C) and Si/Al molar ratio (100150) on the catalyst performance in the dehydration of methanol to dimethyl ether (DME) were studied. The catalystswere characterized by BET, XRD, NH3-TPD, TGA/DTA, and SEM techniques. The full factorialdesign of experiments was applied to synthesis of ZSM-5 zeolite and the effects of synthesisconditions and their interaction on the yield of DME as the response variable were determined. Analysis of variance showed that two variables and their interaction significantly affected the response. According to the experimental results, the optimized catalyst prepared at 170 C andSi/Al = 100 molar ratio showed better performance compared with those prepared at other conditions.

 

 

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